实验技术

高效液相色谱串联质谱法定量检测稻谷中的稻曲病菌毒素A和D

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  • 江苏省农业科学院 江苏省食品质量安全重点实验室/省部共建国家重点实验室培育基地/农业部食品安全监控重点开放实验室, 江苏 南京 210014;

收稿日期: 2011-06-27

  修回日期: 2011-10-14

  网络出版日期: 2012-03-10

基金资助

国家自然科学基金资助项目(30901006);国家重大科技专项(2009ZX08011015B, 2008ZX08011003); 江苏省科技支撑计划资助项目(BE2010757)

Simultaneous Quantitative Determination of Ustiloxin A and Ustiloxin D in Rice  Grains by High Performance Liquid Chromatographytandem Mass Spectrometry

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  • Key Laboratory  of Food Quality and Safety of Jiangsu Province/State Key Laboratory Breeding Base for Jiangsu Province/Key Laboratory  of AgroFood Safety and Quality, Ministry of Agriculture, Jiangsu Academy of Agricultural Sciences, Nanjing 210014, China;

Received date: 2011-06-27

  Revised date: 2011-10-14

  Online published: 2012-03-10

摘要

建立了稻谷中稻曲病菌毒素A和D污染物的高效液相色谱串联质谱的分析方法。该方法简单、灵敏、准确,可同时定量检测稻谷中稻曲病菌毒素A和稻曲病菌毒素D。

本文引用格式

祭芳,曹欢,徐剑宏,殷宪超,史建荣* . 高效液相色谱串联质谱法定量检测稻谷中的稻曲病菌毒素A和D[J]. 中国水稻科学, 2012 , 26(2) : 246 -250 . DOI: 10.3969/j.issn.10017216.2012.02.015

Abstract

A method based on high performance liquid chromatography coupled with tandem mass spectrometry(HPLCMS/MS) was developed for simultaneous determination of  ustiloxin A and ustiloxin D. This method is simple,sensitive and accurate, and can be used for simultaneous quantitative determination of ustiloxin A and ustiloxin D in rice grains.

参考文献

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